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The publication considers the possibility to use the original corn stalks and corn stalks after pyrolysis as raw materials for carbon nanomaterials manufacture. The changes in the properties of corn stalks during pyrolysis have been studied at different temperatures and their influence on the corn stalks properties have been revealed with the use of the ultimate and the X-ray fluorescence analyses. The results of the research are obtained in the form of carbon nanoparticles produced from the above-mentioned stock and pyrolysed corn stalks.